Read e-book online Contemporary Boron Chemistry (Special Publications) PDF

By M. Davidson, A.K. Hughes, T.B. Marder, K. Wade

ISBN-10: 0854048359

ISBN-13: 9780854048359

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Proton N M R spectra of Cp2ZrH{(p-H),BC4H8) at elevated temperatures are shown in Figures (2). The two signals of the bridge hydrogens broaden and coalesce as the temperature is raised. During the process, the signal of the terminal hydrogen also broadens into the baseline. The signal of the Cp hydrogens is also broadened at higher temperature. This behavior is independent of the concentration, which suggests an intramolecular hydrogen exchange among Cp hydrogens, Zr-H terminal hydride, and Zr-H-B bridge hydrogens occurred at elevated temperature.

Lancaster, M. Thornton-Pett, and M. Bochmann, J. Am. Chem. 1998,120,6816. 16. E. Herberich, B. Hessner, W. Boveleth, H. Liithe, R. Saive and L. Zelenka, Angew. Chem. Int. Ed. Engl. 1983,22, 1024; G. E. Herberich, T. Carstensen, N. Klaff and M. Neuschiitz, Chem. Ber. E. J. Eckenrath and U. Englert, Organometallics 1997,16,4292 and 4800. 17. G. JimCnez Pindado, M. Corradi, M. Thomton-Pett and M. Bochmann, unpublished results. 18. The formation of borole complexes from boryldiene precursors has also been observed for C,Me, complexes but could not be isolated: B.

Liu, F. ; Meyers, E. ; Shore, S . G. Inorg. Cheh. 1999, 38,2169. ; Liu, F. ; Shore, S . G. Magn. Reson. Chem. 1998, 36, S145. Organolanthanide Compounds Bearing Versatile Ligands Shaowu Wang and Zuowei Xie* DEPARTMENT OF CHEMISTRY, THE CHINESE UNIVERSITY OF HONG KONG, SHATIN NT, HONG KONG. ' The most popular n ligands used in organolanthanide compounds are cyclopentadienyl and its derivatives. As isolobal analogues to the cyclopentadienyl ligand, C2B10,4 and C2B45 ligand systems have been successively introduced to lanthanide chemistry, resulting in a new class of organolanthanide compounds.

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Contemporary Boron Chemistry (Special Publications) by M. Davidson, A.K. Hughes, T.B. Marder, K. Wade

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